For a constant feeding of sample, we recommend using a Disk Mill PULVERISETTE 13. Because this type of alloy does not seems to be too brittle, we recommend a slower feeding speed of sample.
The alloy of tungsten and rhenium seems to be brittle enough to get ground. A smearing between the disks when sample uses to be ductile was not observed.
With a slower feeding speed ~ 60 g/min, sample can be ground with finest possible gap without problems. About 8 minutes have been needed to grind the 489 g of sample.
Because ground particles only need to be < 100 µm in one dimension, it is possible to find particles with a length of up to 300 µm in the collecting vessel.
To determine the fineness, we used our Vibratory Sieve Shaker ANALYSETTE 3 Pro and sieved an aliquot of sample with the test sieves of 63 µm and 160 µm. Already 37,1 % of sample use to be in the desired range. Still 49,6 % of sample uses to be > 160 µm and might be fed a second time after separation of the desired range.
Also a Vibrating Cup Mill PULVERISETTE 9 might be capable for a batch wise grinding of sample.