A pre grinding of sample is required. For this, we used our Jaw Crusher PULVERISETTE 1. Afterwards, we recommend grinding in suspension with Planetary Mono Mill PULVERISETTE 6 classic line.
With this pre grinding step, sample size will be reduced until a grinding with e.g. Vibration Cup Mill PULVERISETTE 9 or Planetary Mono Mill PULVERISETTE 6 classic line is plausible.
After 2 minutes of grinding, the complete sample has been ground to < 8mm. See following trials for fine grinding.
100 ml grinding set made of hardmetal tungsten carbide (WC)
Feed quantity:
150 g
Feed Size:
< 1 cm
Grinding time:
40 s
Final fineness:
> 1 mm
Comments:
With our Vibration Cup Mill PULVERISETTE 9, sample will mainly become flat out to flakes with a size of ~ 1mm. By longer grinding, sample will become sintered together. A longer dry grinding is not possible.