500 ml grinding bowl made of zirconium oxide (ZrO2)
+ 25x 20 mm Ø ZrO2 grinding balls
Feed quantity:
250 g
Feed Size:
1 mm
Grinding time:
40 min
Final fineness:
d50 < 7.73 µm d90 < 28.96 µm
Comments:
As desired, the sample has been ground with zirconium oxide as bowl and grinding ball material. This way, a discoloration of sample by abrasion will be hindered (grinding with metals for bowl or grinding ball material use to produce gray colored discolorations).
After a total dry grinding time of 40 minutes, the sample starts sticking to bowl and balls.
This uses to happen after the majority of particles reached a fineness of < 20-30 µm. Interacting forces between fine ground particles will become bigger as their own g-force. Therefore, particles will stick to each other and become compressed by the used grinding balls. These clusters of particles also contain bigger particles which will not be ground any further.
A longer dry grinding is not recommended.
A final fineness of d50 < 7,73 µm and d90 < 29,86 µm has been detected with our Laser Particle Sizer ANALYSETTE 22 Compact. The target of grinding 100 % < 50 µm has been reached. A further grinding in suspension (to eliminate interacting forces) is not necessary.