For grinding the sample to < 100µm, we recommend using the Planetary Micro Mill PULVERISETTE 7 classic line with bowls and balls made of sintered corundum.
45 ml grinding bowl made of sintered corundum (Al2O3)
+ 7 x 15 mm ø grinding balls made of Al2O3
Feed quantity:
1,1 g
Feed Size:
15 mm
Additive:
+ 6ml water
Grinding time:
3 min
Final fineness:
< 100 µm (fine paste)
Comments:
Because of fast sticking of sample, we only recommend grinding the sample in suspension. Therefore, we added 6ml of water to the needles and ground for totally 3 minutes.
After 3 minutes of grinding, sample has been ground to a pasty mush with all particles < 100µm.