250 ml grinding bowl made of zirconium oxide (ZrO2)
+ 15x 20 mm ZrO2 grinding balls
Feed quantity:
100 g
Feed Size:
< 0,5 mm (see result 1)
Grinding time:
+ 8 min (∑: 10 min)
Final fineness:
d50<4,5 µm d90<14,7 µm
Comments:
In dry grinding, sample starts sticking after totally 10 minutes. A longer dry grinding time is not recommended.
The sample started sticking to bowl and balls. This uses to happen after the majority of particles reached a fineness of < 20-30µm. Interacting forces between fine ground particles will become bigger as their own g-force. Therefore, particles will stick to each other and just become compressed by the used grinding balls. These clusters of particles also contain bigger particles which will not be ground any further too.
A better endfineness can only be achieved by grinding in suspension.