M090124 | |
Chemistry | |
10µm | |
d50 < 60nm | |
10g | |
With both kinds of samples, the desired fineness could be reached with the Planetary Micro Mill PULVERISETTE 7 premium line within less of 60 minutes. |
Planetary Micro Mill PULVERISETTE 7 premium line1100 rpm |
||
Equipment: |
80 ml zirconium oxide (ZrO2) bowl with 100g of 1 mm ZrO2 balls. |
|
|
Sample: Li-Managanese Phosphate
|
|
|
10 g | |
|
10 µm | |
|
+ 35ml H2O | |
|
60 min*1 | |
|
d50 < 60 nm*2 | |
|
*1: Grinding steps (for all 4 trials!): 5min grinding time + 15min pause.
*2: For measuring in submircon range, Mie-Parameter must be required. We calculated the best fitting values.
See our partice size analysis after 60min with ANALYSETTE 22 NanoTec, on Meas.No 7167. |
|
Download: | 090124_LiMnPO4_60min.pdf |
Planetary Micro Mill PULVERISETTE 7 premium line1100 rpm |
||
Equipment: |
80 ml zirconium oxide (ZrO2) bowl with 100g of 1 mm ZrO2 balls. |
|
|
Sample: Li-Managanese Phosphate
|
|
|
10 g | |
|
10 µm | |
|
+ 35ml H2O | |
|
120 min | |
|
d50 < 25 nm*1 | |
|
*1: For measuring in submircon range, Mie-Parameter must be required. We calculated the best fitting values.
See our partice size analysis after 120min with ANALYSETTE 22 NanoTec, on Meas.No 7166. |
|
Download: | 090124_LiMnPO4_120min.pdf |
Planetary Micro Mill PULVERISETTE 7 premium line1100 rpm |
||
Equipment: |
80 ml zirconium oxide (ZrO2) bowl with 100g of 1 mm ZrO2 balls. |
|
|
Sample: Li-Cobalt Phosphate
|
|
|
10 g | |
|
0,4 µm | |
|
+ 17ml H2O | |
|
60 min | |
|
d50 < 30 nm*1 | |
|
*1: For measuring in submircon range, Mie-Parameter must be required. We calculated the best fitting values.
See our partice size analysis after 60min with ANALYSETTE 22 NanoTec, on Meas.No 7193. |
|
Download: | 090124_LiCo_60min_Mono.pdf |
Planetary Micro Mill PULVERISETTE 7 premium line1100 rpm |
||
Equipment: |
80 ml zirconium oxide (ZrO2) bowl with 100g of 1 mm ZrO2 balls. |
|
|
Sample: Li-Cobalt Phosphate
|
|
|
10 g | |
|
0,4 µm | |
|
+ 17ml H2O | |
|
120 min | |
|
d50 < 31 nm*1 | |
|
*1: For measuring in submircon range, Mie-Parameter must be required. We calculated the best fitting values.
See our partice size analysis after 60min with ANALYSETTE 22 NanoTec, on Meas.No 7261. |
|
Download: | 090124_LiCo_120min.pdf |